煤层气井HPG压裂液低温破胶剂实验优选

Experimental selection of low-temperature gel breaker for HPG fracturing fluid in CBM wells

  • 摘要: 实验室进行了4种不同酸溶液的破胶实验,应用旋转黏度计、马尔文激光粒度仪、离心机、分光光度计等多手段测定了破胶液的黏度、残渣粒径分布、残渣含量及滤液中的含糖量,优选出了适用于低温煤储层的破胶剂。实验测试评价了该破胶液对煤储层的伤害性。结果表明:温度20℃时HXM+NH4Cl复合酸破胶效果好,浓度越大破胶速度越快。使用浓度0.10%HXM+0.05%NH4Cl的酸液进行破胶,2 h内压裂液黏度可降到5 m Pa·s以下,破胶液残渣中值粒径为86μm,残渣含量70 mg/L。原始渗透率小于0.87×10-15m2时,煤芯渗透率的伤害率小于20%;煤储层的原始渗透率越大,破胶液对岩芯的伤害率越大。该复合酸破胶剂与常规氧化破胶剂相比,具有低温下破胶彻底、残渣含量少、伤害轻等优点。

     

    Abstract: Gel breaking experiments about four different acid solutions were conducted,the fracturing fluid viscosity, residue particle size distribution,residua content and sugar content in the gel breaking liquid were separately tested by rotational viscometer,Malvern laser particle size analyzer,centrifuge and spectrophotometer,and the breaker for the low temperature coal reservoir was optimized. The damage ratio of gel breaking liquid to the coal reservoir was evaluated by experimental tests. The results show that:Hydroxyropyl-guar gum fracturing fluids could be broken quickly and com- pletely at the temperature 20 degrees by using the HXM+NH4 Cl,the greater the concentration,the faster the gel break- ing speed;When the concentration is 0. 10% HXM+0. 05% NH4 Cl,the fracturing fluid viscosity can drop less than 5 mPa·s within 2 hours,the residue particle size is 86 μm,residue content is 70 mg / L. The damage ratios of perme- ability by coal samples are lower than 20% when the original permeability is less than 0. 87×10-15 m2 . Furthermore, the higher the original reservoirs permeability,the greater the damage ratio is. Compared with the oxide breaker,the advantages of the composite acid breaker are quite torn glue at low temperature,little residual content and the minor injury.

     

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